Empyrean

  • Radiation:  Copper (default) and cobalt (upon request)

  • Measurements

    • Phase identification

    • Phase quantification

    • Lattice parameters

    • Crystallinity

    • Crystallite Size

    • Microstrain

    • Thermal expansion (in situ HTXRD)

    • Reaction equations (in situ HTXRD)

    • Reaction temperatures (in situ HTXRD)

    • Reaction kinetics (in situ HTXRD)

  • Sample Types​

    • Powder​

    • Solid

    • Thin film

  • Hardware​

    • Incident Side​

      • Parallel beam mirror​

      • Programmable divergence slits

      • Focusing mirror

    • Diffracted Side​

      • Programmable anti-scatter slits​

      • Fixed anti-scatter slits

      • 0.09  parallel plate collimator

    • Sample stages​

      • Reflection/transmission/spinner (default)​

      • Anton Paar HTK 1200N (high temperature)

        • Dry air, ambient air, inert gas, and 10   torr vacuum environments​

      • Programmable XYZ

      • Chi-phi-Z

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X'Pert3 MRD

  • Radiation:  Copper

  • Measurements

    • Phase idendification

    • Lattice parameters

    • Crystallinity

    • Crystallite size

    • Microstrain

    • Texture (aka preferred orientation or pole figures)

    • Residual stress

    • Grazing incidence XRD

    • High resolution XRD

  • Sample Types​

    • Fiber

    • Solid

    • Thin film

  • Hardware​

    • Incident Side​

      • Parabolic mirror​

      • Double crossed slits collimator

      • 4X Ge(220) 4 crystal monochromator

    • Diffracted Side​

      • 0.09  parallel plate collimator​

      • 0.27  parallel plate collimator

      • Rocking curve optic

      • Two bounce asymmetric triple axis analyzer​

    • Sample Stage​

      • 5 axis (chi-phi-X-Y-Z)​ cradle

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More information about possible experiments can be found in Videos: Measurements